The sem is intended to be used as the primary communication path for all alarm signaling to the central monitoring station. The cmi sem leo 1550 is composed of one gemini column cf. Determining phase volume fraction in steels by electron. Leo 1550 field emission scanning electron microscope fesem is an ultrahigh resolution field emission sem utilizing the gemini field emission column.
For ebl experiments, samples were loaded directly into the chamber to be exposed, then removed from the chamber, developed for 90 s in ar 30047 allresist and rinsed in deionized water. A leo 1550 sem at 5 kev was used to investigate the morphology of both precursor and annealed films. The instruments of the evo family combine high performance scanning electron microscopy with an intuitive, userfriendly experience. You can use 4 diferents holder according to the needs cf. Scanning electron microscope sem and focus ion beam fib sem leo 1550 in zone 1 is a very powerful tool to study profiles after. The electron column contains a pressure differential aperture that allows the specimen chamber to be operated at a low or poor.
Sem micrographs were taken using a leo 1550 scanning electron microscope operating at 2 kv with inlens and everhartthornley detectors. Xray setup to set up your system for xray collection, choose xray. Arial arial unicode ms times new roman baskerville default design technical objective slide 2 leo 440i sem leo sem. Tmwave leo range 3 inca wave interfacing manual for leo range 3 page 2.
Wdx spectrometers that may be fitted to one of the sem. The cmi is a complex of clean rooms and processing equipment for the training and scientific experimentation devoted to the users of microtechnologies. This document is an introduction to the operation of the jeol 5800lv scanning electron microscope and the oxford isis 300 analytical system. Semeds leo supra 55 vp standard operating procedure. Xray diffraction xrd panalytical xpert pro alpha1 was used to examine the crystal structure of the nanorods. Manufacturer specifications leo 1550 fe sem, zeiss please note. It is primarily designed to provide high resolution imaging at low and ultralow accelerating voltages 3kev down to 200ev.
This manual should be considered a work in progress. Sem compatibility leo supra 35vp sem leo supra 25 sem leo ultra 55 sem leo 1540 xb db leo 1430 series sem leo 1450 series sem leo 1530 series sem leo 1550 series sem jeol jsm5800 sem jeol jsm6400 sem jeol jsm6500f sem jeol jsm6060 sem hitachi s4500 type 1 sem hitachi s4500 type 2 sem hitachi s4700 type 2 sem hitachi s4800 type 2 sem. Each adobe pdf file encapsulates a complete description of a fixedlayout 2d document that includes the text, fonts, images, and 2d vector graphics which compose the documents. Elemental analysis of collected was conducted using spirit software. Besidestheascastmaterial,plateswereputthroughdifferent homogenisation heat treatments. As opposed to wrought material, cast materials can generally be subjected to homog. In order to gain access on the tool, a formal qualification by staff is required. University of california, berkeley, california, usa. This is a short course presenting the basic theory and operational parameters of the scanning electron microscope sem. Scanning electron microscopy was performed on a leo 1550 fesem keck sem operating at 2.
The scanning electron microscope leo 15xx is a fully computer controlled instrument. Introduction generality the cmi sem leo 1550 is composed of one gemini column cf. Leo software manual is available for download on the sem pc under e. It is well suited to a variety of applications owing to its versatile specimen chamber and large capacity cartesian stage. Scanning electron microscopes sem scan a sample with a focused electron beam and get images with information about the samples topography and composition. Manual do operador colheitadeiras 1450, 1550, 1450 cws, 1550 cws, 1450 wts e 1550 wts.
Providing for up to 8 multiplexes of processing functionality in a single ru package, the sem significantly lowers the barrier to entry in an ondemand environment. Manual point counting was performed using a twodimensional systematic point count with a finemesh lattice. The zeiss gemini 500 scanning electron microscope sem takes the best capabilities of the keck sem and enhances them. Info the zeiss leo 1550vp is a fully pc controlled sem. Samples prepared for sem were analyzed by an edx detector attachment for the leo 1550 sem at up to 20 kv accelerating voltage, using a 60. The height of the resulting structures was determined by laser scanning pro. Leo 1550 sem elphy quantum nanolithography system 60 min ebeam.
All operations, settings and functions are controlled by use of a key board, a mouse and a joystick. This instruction manual is designed for users who have been trained to operate the workstation. Reservation names must correspond to the operators. In the sem this functionality is connected with the green. The end result was the sem 35 manpack, the sem 25 vehicle transceiver and the em25 vehicle receiver. The german contract was awarded to standard elektrik lorrenz ag of stuttgart. Sem images of the assynthesized gan nw arrays are shown in figure 1a,b. Only minimal tightness is needed to seal up to 700 bar. Sem eds instruction manual doubleclick on the spirit icon on the desktop to start the software program. Instructions for use of zeiss 1550vp field emission sem. Page 18 there is a defect in the braking coil or in the cabling. Zeiss software manual is available for download on the sem pc under e.
The geminisem family stands for effortless imaging with subnanometer resolution. With time, we will add sections as operating procedures are developed or improved by user experience. None of the equipment posted for sale on is owned by medwow, should you have any questions regarding a specific item, please direct them to the appropriate seller by making use of the available communication channels on the items page. M aperture, with a working distance of 15 mm at a 15 takeoff angle. All maintenance should follow the procedures set forth in the manufacturer. Fabrication of lowdensity, lowdisorder samples for. Instructions for use of zeiss 1550vp field emission sem with. The electron scanning microscope sem, leo 1550 images are taken before next process. Keep the instruction manual nearby the workstation and hand it over to future owners of the instrument. Funksprechgeratsatz sem 52 teil 4 f feldinstandsetzung radio set sem 52 part 4 f field maintenance low level maintenance, including exchanging parts and measuring performances. The scanning electron microscopes produce high magnification images with high resolution, a feature of which makes them suitable tools for a wide range of applications in.
All ebsd experiments were performed using a leo 1550 sem with a schottky field emission gun operating at 20 kv. Scanning electron microscopy sem and energy dispersive xray analysis edx were carried out with a leo 1550 field emission sem fesem. In order to increase the inplane electrical conductivity of the vacnts without losing the intrinsic vertical alignment of the individual nanotubes, a layer of ni was dc sputtered. Invacare leo service manual replace scooter none drive motor see replacing the judders in motors defective drive motor on page drive mode replacing the drive lever see replacing the potentiometer potentiometer potentiometer on page defective replace. Scanning electron microscopy sem is a test process that scans a sample with an electron beam to produce a magnified image for analysis. Figure 2, one process chamber with a motorized stage on 5 degree of freedoms x, y, z, tilt and. Electronic change of the ais aperture with aperture selection by the user manual. Testing work repair instructions this manual is part of the instructions for use.
Home housed in ictas crc, the nanoscale characterization and fabrication lab is an instrumentation facility for researchers technology is at a unique point in history. Figure 2, one process chamber with a motorized stage on 5 degree of freedoms x, y, z, tilt and rotation and one airlock. This manual contains information on limitations regarding product use and function and information on the limitations as to liability of the manufacturer. Menu manual for alcatel a601 e university of notre dame. Georgia institute of technology grants and contracts. Voltage is normally set as 5kv for imaging and 15kv for compositional edx analysis. Semeds leo supra standard operating procedure version.
Leo 2 has 716 unf male thread and is delivered complete with an oring seal swivel fitting which allows leo 2 to be rotated through 360. Eros eros scelerisque ut nullam condimentum torquent ad feugiat faucibus nulla a a inceptos elementum aliquam vestibulum velit platea condimentum massa sem sapien. Xray functions access the basic xray acquisition, display a nd analysis functions through either the xray menus or the xray toolbars. Zeiss geminisem field emission scanning electron microscope. The micrograph was taken by volker brinkmann with a leo 1550 scanning electron microscope. Instructions for use of leo 1550vp field emission sem with oxford eds and hkl ebsd.
Cornell center for materials research leo 1550 fesem. The shaft and flange have been coated with a rust inhibitor. Any damage found should be reported immediately to sem and the carrier. Sem manual click on the downloadable files tab to download the pdf file.
Oxford instruments energydispersive spectroscopy eds. Scelerisque nulla in ad id vitae cras adipiscing leo neque magnis justo semper a venenatis a nam adipiscing a senectus feugiat adipiscing suspendisse consectetur elit id euismod a. Zeiss leo 1550 fe sem electron microscope for sale. Zeiss leo 1550 fesem electron microscope manufacturer. Ccmr shared facilities comply with cornell regulations, applicable federal, state, and local regulations, university health and safety board requirements, and other university health and safety standards, detailed in the pdf below. Dec 11, 2010 these adverts are supporting the forums costs and the productsservices are not endorsed by the forum owners. The scanning electron microscope sem facility comprises a carl zeiss leo 1450vp sem. The gemini optical column consists a beam booster, inlens detectors and a. Photovoltaic measurements were recorded employing a solar simulator 300 w model 91160, newport with an am 1. Imaging is achieved using both secondary and backscattered electrons, to produce topographical and or compositionalbased images.
Scanning electron microscopy, sem analysis laboratory. None of the equipment posted for sale on is owned by medwow, should you have any questions regarding a specific item, please direct them to the appropriate seller by making use of. More detailed then most field maintenance manuals, but alas no detailed schematics. Csems conventional sems with a thermic electron source and fesems field emission sems with a field emission electron source from zeiss deliver high resolution imaging and superior. Sem dc brushed servomotors are rated for the temperature rises specified in nema standard mg1 part 12. Figure 2, one process chamber with a motorized stage on 5.
Highly flexible, all solidstate microsupercapacitors from. The stem images were acquired on a fei tecnai f20 with a schottky field emission gun operating at 200 kv. Zno nanotubebased dyesensitized solar cell and its. Make sure the specimen holder with samples fixed is ready. The jeol 5800 sem is a sophisticated scanning electron microscope that was designed to operate in either high or low vacuum the lv connotation indicates the presence of the low vacuum controls.
Samples were prepared by adsorption onto a silicon wafer, which was then attached to a flat aluminum platform sample holder. Comparative characterization methods for metal oxide. All ebeam patterning was performed using a zeiss leo 1550 sem that we modified for oir, which is equipped with a raith elphy quantum lithography system. This manual is designed for users operators who have been trained in the use of the instrument by an. Pc1500 1550 user manual portuguese classicseries 6 zone alarm control panel pc1550 pc1500pc1550 installation manual french classicseries 6 zone alarm control panel. All operations, settings and functions necessary for the handling of the. Ccmr shared facility policies cornell center for materials. User fees are charged to all users to offset the costs incurred in providing scientific equipment and technical. Structural equation modeling is a way of thinking, a way of writing, and a way of estimating. Application of plasma cleaning technology in microscopy evactron. Tescan sem solutions scanning electron microscopy is a wellknown nondestructive technique that uses an electron beam probe to analyse samples surface down to nanoscale. Instructions for use of leo 1550vp field emission sem caltech gps. This is a stepbystep operation manual written for the zeiss supra40 scanning electron microscope at the university of texas at dallas cleanroom, including. Evo can be tailored precisely to your requirements, whether you are in life sciences, material sciences, or routine industrial quality assurance and failure analysis.
Portable document format pdf is a file format created by adobe systems for document exchange. Scanning electron microscope operation zeiss supra40 roger robbins 9102010 update. The leo zeiss 1550 is a highperformance schottky fieldemission sem capable of resolution in 25 nm size range. The sulfur content of the films was measured with eds at 20 kev, in a leo 440 scanning electron microscopy sem with an edax system. Thickness measurements were made with a veeco dektak 150 profilometer. The method is also known as sem analysis and sem microscopy, and is used very effectively in microanalysis and failure analysis of solid inorganic materials. Tuv gs this product complies with ul31111, cancas c22. Semv8 edge encryptor modulator 507199001 ac product. Reprint of the earlier july 1978 manual, including changes 1 and 2. Providing highspeed interfaces to servers and content aggregation systems, the sem performs multiplex creation, encryption,64256qam modulation and upconversion across the full hfc. The system enhancement module sem can be used with dsc powerseries pc1616, pc1832, and pc1864 panels to enable wireless reporting of alarms and other system events using the cdma, hspa, or lte wireless cellular network.
428 699 1326 1318 666 591 1380 664 425 154 614 1268 720 1035 347 1553 516 1402 599 799 1454 802 1542 815 1309 515 974 422 503 1010 805 1218 459 1218 980 992 1420 817 823 715